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The development of flupyradifurone residue determination method in rapeseeds and rape oil

Abstract

The method of flupyradifurone residue determination in rapeseeds and rape oil is introduced in the article. The sample preparation is based on extraction of analyte with acetonitrile followed by cleaning up in a system of immiscible liquids and solid phase extraction. Residues determination was carried out by ultra high performance liquid chromatography with diode array detector. The limit of quantification is 0,02-0,05 mg/kg.

About the Authors

A. V. Bykovsky
RUE «Institute of Plant Protection»
Belarus

a/c Priluki, Minsk district



A. O. Poddubnaya
RUE «Institute of Plant Protection»
Belarus

a/c Priluki, Minsk district



References

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7. Гигиенические нормативы содержания действующих веществ пестицидов (средств защиты растений) в объектах окружающей среды, продовольственном сырье, пищевых продуктах: постановление Министерства здравоохранения Республики Беларусь, 27 сент. 2012 г., № 149. // Законодательство / Центр экологических услуг [Электронный ресурс]. – Режим доступапа: http://www.iso14000.by/library/low/industry/376. – Дата доступа: 12.05.2015.


Review

For citations:


Bykovsky A.V., Poddubnaya A.O. The development of flupyradifurone residue determination method in rapeseeds and rape oil. Plant Protection. 2017;(41):280-286. (In Russ.)

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ISSN 0135-3705 (Print)