The development of flupyradifurone residue determination method in rapeseeds and rape oil
Abstract
The method of flupyradifurone residue determination in rapeseeds and rape oil is introduced in the article. The sample preparation is based on extraction of analyte with acetonitrile followed by cleaning up in a system of immiscible liquids and solid phase extraction. Residues determination was carried out by ultra high performance liquid chromatography with diode array detector. The limit of quantification is 0,02-0,05 mg/kg.
About the Authors
A. V. BykovskyBelarus
a/c Priluki, Minsk district
A. O. Poddubnaya
Belarus
a/c Priluki, Minsk district
References
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Review
For citations:
Bykovsky A.V., Poddubnaya A.O. The development of flupyradifurone residue determination method in rapeseeds and rape oil. Plant Protection. 2017;(41):280-286. (In Russ.)